The Journal of
the Korean Journal of Metals and Materials

The Journal of
the Korean Journal of Metals and Materials

Monthly
  • pISSN : 1738-8228
  • eISSN : 2288-8241

Editorial Office


  1. 부산대학교 재료공학과 (School of Materials Science and Engineering, Pusan National University, Busan 46241, Republic of Korea)
  2. 부산대학교 소재기술연구소 (Institute of Materials Technology, Pusan National University, Busan 46241, Republic of Korea)
  3. ㈜제이비랩 (R&D Center of JB Lab Corporation, Seoul 08788, Republic of Korea)



Laser frequency, Laser-induced forward transfer, Microchip transfer, Process optimization, Transfer yield

1. INTRODUCTION

Micro-LED technology is widely considered one of the most promising candidates for next-generation display systems[1- 4]. Compared with conventional liquid crystal display (LCD) and organic light-emitting diode (OLED) technologies, micro-LEDs offer several key advantages, including high brightness, improved energy efficiency, and excellent thermal and operational stability[5]. As micro-LEDs are based on inorganic semiconductor materials rather than organic emissive layers, they can achieve higher luminance and longer device lifetimes. In addition, each micro-LED chip functions as an individual pixel, enabling extremely high-resolution displays with superior reliability[2].

Owing to these advantages, micro-LED technology has attracted increasing interest for a wide range of applications, such as large-area televisions, wearable devices, automotive displays, and emerging augmented reality systems[6]. Despite these advantages, several technical challenges remain before micro-LED displays can be fully commercialized[7].

One of the most critical challenges is the mass transfer of the microscale LED chips from the growth wafer to the target substrate[8]. In typical micro-LED fabrication processes, individual LED chips are first fabricated on an epitaxial wafer and then transferred to a display backplane[5].

For large-area displays, this process requires the accurate placement of millions of microdevices. Consequently, the transfer process must achieve both high alignment precision and high throughput, while maintaining excellent process reproducibility[9].

Various microdevice transfer approaches have been explored to address this issue, including elastomer stamp transfer, electrostatic transfer, and fluidic self-assembly. Among these approaches, laser-induced forward transfer (LIFT) has emerged as a promising technique owing to its noncontact nature and high spatial precision[10]. In the LIFT process, pulsed laser irradiation generates localized energy at the interface of the donor substrate, enabling the forward transfer of materials or devices toward the receiver substrate[11, 12]. As the transfer process can be controlled by adjusting the laser parameters, LIFT has been investigated as a potential method for microdevice assembly and micro-LED transfer applications[13].

Laser-based transfer techniques have been extensively studied for microscale device assembly and material processing[14]. Early LIFT studies mainly focused on transferring functional materials, such as metals, polymers, and inks, to form micropatterns or electronic structures[15, 16]. As the technology progressed, LIFT began to be applied to the transfer of microdevices and semiconductor components. More recently, several studies have explored the use of LIFT for micro-LED device transfer, demonstrating that laser-driven processes can enable the precise positioning of microscale devices and offer a potential route for large-area device integration[17, 18].

However, many previous studies have focused on demonstrating the feasibility of device transfer under specific experimental conditions[10]. Systematic investigations of the process parameters and their influence on transfer behavior remain relatively limited[19]. In addition, most studies have been conducted using a single device size or within a narrow process window, making it difficult to establish reliable process references for practical applications. From a manufacturing perspective, micro-LED display production requires a transfer process that can achieve both high yield and practical throughput[19]. As the display resolution increases, the number of microdevices required for a single panel significantly increases. Therefore, even a small reduction in transfer yield can result in substantial production losses. Establishing a robust and scalable transfer process is essential to bridge the gap between laboratory-scale demonstrations and practical micro-LED manufacturing technologies.

In this study, we investigate a systematic approach for LIFT-based microchip transfer by integrating temporal and spatial energy considerations. This study analyzes the relationship between laser frequency, temporal irradiation condition, and effective energy delivery to examine the effect of frequency on transfer behavior.

In addition, the geometric relationship between the laser spot size and chip size is introduced as a key parameter governing the spatial energy distribution, enabling stable transfer behavior under the tested chip-size conditions. Based on these considerations, optimized process conditions are experimentally identified and validated under the present experimental conditions for microchips with sizes ranging from 30 to 70 µm, achieving transfer yields exceeding 99% with high reproducibility. These results provide useful insights into the relationship between process parameters and transfer behavior. The findings suggest that appropriate control of temporal and spatial parameters can serve as a useful practical reference for optimizing LIFT-based microchip transfer under similar experimental conditions.

2. EXPERIMENTAL

Silicon microchips with lateral sizes ranging from 30 to 70 µm were prepared on a glass carrier coated with a polyimide-based dynamic release layer (DRL). The DRL thickness was controlled to approximately 1 µm based on previously reported blister-driven transfer conditions under similar UV laser irradiation environments[12].

A PDMS substrate was used as the receiver, and no intentional gap was introduced between the donor and receiver substrates during the transfer process. Blister-driven transfer was performed using a pulsed ultraviolet (UV) laser with a wavelength of 355 nm.

The laser frequency was varied in the range of 100–260 kHz, while the pulse duration was fixed at 3.8 μs based on the laser system setting. The pulse energy was maintained at approximately 23.5 µJ under the present experimental conditions, while the effective energy density varied depending on the spot size condition[12]. Although the main frequency analysis was conducted within the range of 100–260 kHz, an additional low-frequency condition at 50 kHz was examined for the 70-µm chips to investigate the effect of increased temporal energy delivery under larger chip conditions.

The frequency and spot size were systematically varied to investigate their effects on the transfer stability. The spot-to-chip size ratio was adjusted by controlling the irradiation condition, resulting in different spot sizes relative to the chip size.

Laser scanning was performed under single-exposure conditions at a fixed scanning speed of 500 mm/s. During the experiments, only one parameter was varied at a time, while all other process parameters were kept constant.

The transfer yield was evaluated based on positional alignment and structural integrity after transfer. Reproducibility was assessed through five repeated trials under identical process conditions.

3. RESULTS AND DISCUSSION

3.1. Operational Frequency Window

Laser frequency is a key parameter governing the stability of LIFT processes[20]. In scanning-based LIFT systems, the transfer behavior is strongly governed by the temporal delivery of the laser energy to the chip. Among the various parameters, the laser frequency directly determines the number of pulses interacting with the chip during the scanning process, making it a critical factor for controlling energy accumulation and transfer stability[21].

In scanning-based LIFT systems, the effective interaction between the laser beam and an individual chip is determined not only by the laser energy but also by the number of laser pulses interacting with the chip during the scanning process[19].

Therefore, the frequency directly controls the temporal energy delivery and plays a critical role in determining transfer stability[21]. Under the scanning conditions, the effective interaction time between the laser beam and a single chip can be approximated as

(1)
$t = \frac{L}{v}$

The interaction time determines the duration for which a single chip is exposed to the laser beam during scanning, which directly affects the total energy delivered to the chip[20]. In Eq. (1), L is the chip size and v is the scanning speed. The scanning speed was fixed at 500 mm/s, and the chip size used in this analysis was 50-μm. This approximation is widely used to describe the laser–material interaction time in scanning laser systems. For the present experimental conditions, the chip size was $L = 50$ µm and the scanning speed was $v = 500$ mm/s, resulting in an interaction time of

(2)
$t = \frac{0.05}{500} = 1.0 \times 10^{-4} s$

The interaction time determines the number of laser pulses that interact with a single chip during scanning[10].

The number of laser pulses interacting with a chip can therefore be expressed as

(3)
$N(f) = ft = f \frac{L}{v}$

This indicates that increasing the frequency increases the number of pulses contributing to the energy delivery, thereby potentially increasing the total energy supplied to the chip[10]. In Eq. (3), $f$ represents the laser frequency. Increasing the frequency increases the number of pulses delivered to the chip. To describe the temporal irradiation condition, a dimensionless parameter is defined as

(4)
$\delta(f) = f\tau$

where τ is the effective laser irradiation duration. In this study, τ was set to 3.8 μs based on the laser system setting. As the frequency increases, the fraction of laser-on time within a given period also increases, which may lead to enhanced energy accumulation within the dynamic release layer. This accumulated energy can influence the thermal response of the release layer and affect the transfer behavior. Based on these considerations, a simplified phenomenological expression was introduced to qualitatively describe the competing effects between effective pulse delivery and excessive temporal overlap during the transfer process:

(5)
$S(f) = N(f)[1 - \delta(f)]$

In this expression, the term (1 − δ(f)) represents the reduction in transfer stability caused by excessive temporal irradiation and thermal accumulation at high frequencies. Therefore, transfer stability can be influenced by the balance between sufficient pulse delivery and excessive temporal irradiation or energy accumulation, which can lead to thermal damage. Substituting the expressions for $N(f)$ and $\delta(f)$ defined in Eqs. (1)(3), the expression can be rewritten as

(6)
$S(f) = (\frac{fL}{v})(1 - f\tau)$

Because $L/v = 10^{-4}$ under the present experimental conditions, Eq. (6) can be simplified as

(7)
$S(f) = 10^{-4}f(1 - f\tau)$

To estimate a characteristic frequency, the derivative of the expression is calculated as

(8)
$\frac{dS}{df} \propto 1 - 2\tau f$

Setting the derivative to zero yields a characteristic frequency

(9)
$f^* = \frac{1}{2\tau}$

For the pulse duration used in this study ($\tau = 3.8$ µs), a characteristic frequency can be estimated as

(10)
$f^* \approx 132 kHz$

To compare with this simplified analysis, transfer experiments were conducted at frequencies of 100, 150, and 260 kHz under a fixed scanning speed of 500 mm/s with no intentional gap between the donor and receiver substrates. A pulsed UV laser (λ = 355 nm) with a pulse duration of 3.8 μs was used, and all other process parameters were kept constant during the experiments. Under these fixed conditions, at 100 kHz, the δ value was relatively small ($\delta = 0.38$), resulting in insufficient pulse delivery to sustain stable transfer.

This resulted in unstable transfer behavior and reduced yield. At 260 kHz, the δ value approached unity ($\delta \approx 0.99$), indicating excessive temporal irradiation. In this regime, energy accumulation becomes dominant, reducing the transfer stability and transfer yield. By contrast, the highest transfer yield and most stable transfer behavior were observed at 150 kHz.

This frequency is close to the characteristic value estimated from the simplified analysis (f* ≈ 132 kHz), indicating that the experimentally observed optimum at 150 kHz is generally consistent with the trend suggested by the simplified analysis. The discrepancy between the estimated characteristic frequency and the experimentally observed optimum is attributed to the simplified nature of the phenomenological model. The model does not account for factors such as spatial beam nonuniformity, thermal diffusion within the DRL, pulse-to-pulse thermal accumulation, and material-dependent absorption behavior. Although only three representative frequencies were examined in this study, the results suggest that an intermediate frequency condition provides more stable transfer under the present experimental conditions. This suggests a practical guideline for selecting appropriate frequency conditions under similar experimental setups[22].

Furthermore, the results highlight that frequency is intrinsically coupled with temporal energy accumulation and that a narrow process window exists for stable transfer. From a process perspective, these results suggest that transfer behavior is influenced by the balance between pulse number and temporal irradiation condition. This provides a useful practical reference for selecting appropriate frequency conditions under similar experimental setups.

Fig. 1. (a) Schematic of the LIFT process. (b) 2D optical image of the 50-µm chip LIFT experiment. (c) Number of transferred chips as a function of laser frequency. (d) Number of successfully transferred chips excluding defects as a function of laser frequency. (e) Transfer yield as a function of laser frequency. (f–h) Optical microscopy images of the transfer results at 100, 150, and 260 kHz.

../../Resources/kim/KJMM.2026.64.7.618/fig1.png

3.2. Spot-to-Chip Size Ratio

For the 70-µm chips, this larger chip size naturally requires a higher amount of energy to initiate transfer compared to the 50-µm case. From a physical perspective, the total delivered energy and spatial distribution of energy across the chip play a critical role in determining the transfer stability[22]. Therefore, the spot size relative to the chip size is an important parameter for controlling the energy distribution. Based on the relationship derived in Section 3.1, the initial experiments were performed at 50 kHz under the focused condition (i.e., zero defocus distance, where the laser focal plane coincides with the PI layer surface). However, under this condition, most of the chips were severely burned and stable transfer was not achieved. This result suggests that increasing the delivered energy alone does not lead to a stable transfer[23]. Instead, the manner in which the energy is distributed over the chip area becomes increasingly critical, especially as the chip size increases.

To address this issue, the spot size was increased to reduce the effective energy density applied to the chip. To describe this effect, the spot-to-chip size ratio was defined as

(11)
$\alpha = \frac{D_{spot}}{D_{chip}}$

where $D_{spot}$ is the laser spot diameter and $D_{chip}$ is the chip size. This ratio provides a normalized parameter that describes how the laser energy is spatially matched to the chip geometry under the present experimental conditions. When the spot size was approximately 43 µm, some of the chips were transferred, but most still showed thermal damage similar to the focused condition. The transfer behavior in this regime was not uniform, indicating that the energy distribution across the chip remained uneven. This indicates that a locally concentrated energy distribution can lead to partial damage even when the total delivered energy is sufficient for transfer. As the spot size was increased to approximately 51 µm, the transfer behavior noticeably changed. Most of the chips were transferred without visible damage, and the transfer yield exceeded 95%[9]. Under these conditions, the energy appeared to be distributed more evenly across the chip, avoiding a local energy concentration. The corresponding ratio was

(12)
$\alpha = \frac{51}{70} \approx 0.73$

This result suggests that stable transfer was achieved under the present 70-µm chip conditions when the spot size became comparable to the chip size, ensuring a more uniform spatial energy distribution. When the spot is too small, the energy is concentrated in a limited region, leading to damage[9]. However, when the spot size is increased, the energy spreads over a wider area, allowing for a more uniform interaction with the chip. Therefore, the spot-to-chip ratio can be considered as a useful parameter that governs the balance between energy concentration and distribution across the chip surface. Thus, the spot-to-chip ratio provides a simple method for describing how well the laser energy matches the chip geometry.

These results suggest that a ratio of approximately 0.7 was found to provide stable transfer under the present experimental conditions[22]. It should be noted that the α ≈ 0.73 condition was derived specifically from the 70-µm chip experiments under the present process conditions. Therefore, this value should be regarded as a practical reference rather than a universal criterion. It should be noted that this observation is based on the tested chip size (70 μm) and experimental conditions used in this study. From a process perspective, this parameter is useful because it can be used as a practical reference for similar chip sizes under comparable experimental conditions.

Fig. 2. (a–c) Optical microscopy images for spot sizes of 40, 43, and 51 µm. (d) Optical microscopy image used for single spot size measurements. (e) Schematic of the spot-size-to-chip-size experiment. (f) Percentage ratio of the spot size to the chip size. (g) Number of transferred chips as a function of the spot size. (h) Transfer yield as a function of the spot size.

../../Resources/kim/KJMM.2026.64.7.618/fig2.png

3.3. Optimization Results for Different Chip Sizes

Based on the optimized conditions identified from the frequency and geometric considerations discussed in the previous sections, transfer experiments were carried out for chip sizes of 30, 50, and 70-µm. This experiment was designed to verify whether the optimized conditions could be applied under the tested chip-size conditions, which is important for practical applications. Overall, stable transfer behavior was observed across all chip sizes. The transfer yield exceeded 99% in all cases[24]. Even for the larger 70-µm chips, a reasonably high yield was maintained once the spot size was properly adjusted[25, 26].

This further confirms that spatial energy distribution plays a dominant role in maintaining the transfer stability of larger chips. It should be noted that the 30-µm chips showed stable transfer behavior under conditions similar to those used for the 50-µm chips. For the 30- and 50-µm chips, stable transfer was also achieved under comparable spatial energy distribution conditions, although the corresponding α values were not independently optimized.

This suggests that, under the present experimental conditions, the transfer process becomes less sensitive to the absolute chip size once the energy distribution condition is satisfied. This can be attributed to the spatial energy distribution of the laser beams. Because the spot size is larger than the chip size, sufficient energy is delivered to the entire chip area, whereas the Gaussian profile prevents excessive energy concentration in specific regions.

Another factor that contributes to stable transfer is the spacing between neighboring chips. Because the chips were sufficiently separated, thermal or mechanical interactions between adjacent chips were minimized. This indicates that interchip interference is negligible under the current process conditions, allowing for independent and uniform transfer behavior across the array. As a result, each chip behaves independently during the transfer process, which helps to maintain uniformity across the array.

Collectively, these results suggest that the optimized conditions were applicable to the tested chip sizes. The transfer behavior showed a similar trend across the tested chip sizes, governed by the balance between energy delivery and its spatial distribution.

It should be noted that these observations are limited to the tested chip sizes (30–70 μm) and experimental conditions used in this study.

In practical terms, these results indicate that similar transfer behavior can be achieved for the tested chip sizes by appropriately adjusting the process conditions. This suggests that the relationship between frequency and spot-to-chip size ratio can be used as a useful reference for process optimization under comparable experimental conditions.

Fig. 3. (a–c) Optical microscopy images of the optimized transfer results for chip sizes of 30, 50, and 70 µm, respectively. (d) Schematic of the chip-size-dependent transfer experiment. (e) Number of transferred chips as a function of chip size. (f) Transfer yield as a function of chip size.

../../Resources/kim/KJMM.2026.64.7.618/fig3.png

3.4. Process Reproducibility Evaluation

Process reproducibility was evaluated to determine whether the optimized LIFT conditions could maintain stable transfer behavior under repeated operations. Reproducibility is an important requirement for reliable process operation because consistent performance under identical conditions directly determines process reliability[27, 28]. In practical applications, achieving a high yield in a single experiment is insufficient, and the process must consistently reproduce the same performance under identical conditions[29]. Transfer experiments were repeated five times under the optimized conditions using 50-µm chips. Across all repetitions, the transfer behavior remained highly consistent with no noticeable variation in chip alignment or structural integrity. This indicates that the process is robust against minor fluctuations in the experimental conditions. Moreover, the transferred chips exhibited uniform positioning and stable transfer characteristics, further confirming the stability of the transfer behavior under the same conditions[8]. This low variation demonstrates that the optimized process operates within a stable process window. Similarly, the number of successfully transferred chips showed a negligible deviation across repetitions. These results demonstrate that the optimized process provides highly stable and repeatable performance. Figure 4(c) schematically summarizes the relative influence of the investigated process parameters based on the experimentally observed transfer trends. The ranking is intended as a qualitative interpretation rather than a quantitative statistical analysis. Analysis of the process parameter contributions further revealed that frequency most significantly influenced the transfer stability, followed by the spot-to-chip size ratio and chip size. This hierarchy indicates that temporal energy control plays a dominant role, whereas spatial and geometric factors provide additional stabilization. In particular, the chip size influences the energy distribution required for stable transfer. Larger chips require a broader and more uniform energy profile, which makes them more sensitive to spatial energy conditions. This observation is consistent with the results presented in Section 3.3, where stable transfer across different chip sizes was achieved only when the spot size was appropriately scaled relative to the chip size.

From a physical perspective, the high reproducibility can be attributed to the fact that both the temporal and spatial energy conditions are maintained within a stable operating window. Because the balance between pulse delivery and energy distribution is preserved, the transfer behavior remains consistent across repeated trials.

These results demonstrate that the optimized conditions enable stable and repeatable transfer behavior. More importantly, the results confirm that the transfer process is governed by the coupled effects of the temporal parameters, spatial energy distribution, and geometric scaling. These observations provide useful insights for understanding the transfer behavior under the present experimental conditions. From a practical perspective, this reproducibility is important for achieving consistent transfer behavior under repeated operations[30, 31].

Fig. 4. (a) Schematic of the reproducibility experiment. (b) Optical microscopy image of the reproducibility experiment results. (c) Relative importance of the process parameters considering their effect on the transfer yield. (d) Transfer yield as a function of repeated experiments. (e) Number of transferred chips as a function of repeated experiments.

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4. CONCLUSIONS

Reliable process conditions are important for stable LIFT-based microchip transfer in highly integrated microelectronic applications. In this study, the transfer behavior was investigated by considering the combined effects of geometric and energy-density-related parameters for chips of different sizes (30, 50, and 70 µm). First, the effect of laser frequency on transfer behavior was examined, and the results showed that an intermediate frequency condition provided stable transfer under the present experimental conditions. Subsequently, the influence of the spot-to-chip size ratio on transfer yield was analyzed, indicating that appropriate spatial energy distribution is critical for achieving stable transfer.

Under the optimized conditions identified in this study, transfer yields exceeding 99% were achieved for all tested chip sizes. In addition, reproducibility was evaluated through repeated transfer experiments using 50-µm chips, where consistent transfer performance with minimal variation was observed. These results demonstrate that stable and repeatable transfer behavior can be achieved by appropriately controlling both temporal and spatial process parameters. Overall, this study provides useful insights into the relationship between process parameters and transfer behavior in LIFT processes. The findings suggest that the combined control of laser frequency and spot-to-chip size ratio can serve as a useful practical reference for optimizing LIFT-based microchip transfer under comparable experimental conditions and within the tested chip-size range.

ACKNOWLEDGEMENT

This work was financially supported by the Ministry of Trade, Industry & Energy of Korea (Grant No. 00269589).

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