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Recovery of Palladium Metal with High Purity by Selective Reduction from Inorganic Acid Leaching Solutions of Cemented Zinc
아연치환체의 무기산 침출액에서 선택적 환원에 의한 고순도 팔라듐금속의 회수
Si Jeong Song, Viet Nhan Hoa Nguyen, Man Seung Lee
송시정, Viet Nhan Hoa Nguyen, 이만승
Korean J. Met. Mater. 2022;60(11):837-844.   Published online 2022 Oct 31
DOI: https://doi.org/10.3365/KJMM.2022.60.11.837

Abstract
A small amount of Pd(II) present in spent electroplating solutions is concentrated by cementation. In this work, a process was developed to recover pure palladium metal by selective reduction from the hydrochloric and the sulfuric acid leaching solutions of cemented zinc. For this purpose, hydrazine and ascorbic acid were employed..... More

                   Web of Science 1  Crossref 1
Effect of Ethylene Glycol on the Dissolution of Palladium with HCl Solution Containing Oxidizing Agents and Selective Precipitation of Pd(IV) Compound
Viet Nhan Hoa Nguyen, Si Jeong Song, Man Seung Lee
Korean J. Met. Mater. 2022;60(7):502-510.   Published online 2022 Jun 3
DOI: https://doi.org/10.3365/KJMM.2022.60.7.502

Abstract
There is growing interest in the recovery of pure palladium (Pd) compound from cemented Pd from spent electroplating solutions due to increasing demand for Pd, and there is considerable motivation to develop an efficient recovery process. In conventional methods of leaching Pd metal, HCl solutions containing oxidizing agents are employed...... More

                   Web of Science 4  Crossref 4
Separation of Pd(II) and Zn(II) by Solvent Extraction using Commercial Extractants from Hydrochloric Acid Leaching Solution of Cemented Pd from Spent Electroplating Solutions
도금폐액에 함유된 팔라듐의 아연치환물 염산침출액에서 상용화추출제를 이용한 용매추출로 팔라듐(II)과 아연(II)의 분리
Si Jeong Song, Viet Nhan Hoa Nguyen, Man Seung Lee
송시정, Viet Nhan Hoa Nguyen, 이만승
Korean J. Met. Mater. 2022;60(3):188-197.   Published online 2022 Feb 8
DOI: https://doi.org/10.3365/KJMM.2022.60.3.188

Abstract
The demand for palladium (Pd) has increased and this has made it necessary to recover pure Pd from diverse secondary resources. To recover the small amount of Pd(II) present in spent electroplating solutions, Pd(II) is concentrated by cementation with zinc metal. In this work, a hydrometallurgical process consisting of leaching..... More

                   Web of Science 3  Crossref 4
Separation of Pd(II) and Zn(II) from Sulfuric Acid Solution by Commercial Extractants
황산용액에서 상용화 추출제에 의한 팔라듐(II)과 아연(II)의 분리
Si Jeong Song, Viet Nhan Hoa Nguyen, Man Seung Lee
송시정, Viet Nhan Hoa Nguyen, 이만승
Korean J. Met. Mater. 2022;60(2):132-140.   Published online 2022 Jan 12
DOI: https://doi.org/10.3365/KJMM.2022.60.2.132

Abstract
Spent electroplating solutions contain a small amount of Pd(II). This Pd(II) can be concentrated by cementation with zinc metal powder. In order to recover pure palladium, a hydrometallurgical process consisting of leaching followed by solvent extraction was developed in this work. First, suitable extractants for the selective extraction of Pd(II)..... More

                   Web of Science 2  Crossref 2
Leaching of a Mixture of Palladium and Zinc Metal Using Hydrochloric and Sulfuric Acid Solutions
염산과 황산용액에서 팔라듐과 아연 금속혼합물의 침출
Si Jeong Song, Viet Nhan Hoa Nguyen, Man Seung Lee
송시정, Viet Nhan Hoa Nguyen, 이만승
Korean J. Met. Mater. 2021;59(7):469-475.   Published online 2021 Jun 16
DOI: https://doi.org/10.3365/KJMM.2021.59.7.469

Abstract
Spent electroplating solutions contain small amounts of Pd(II). Cementation of Pd(II) with zinc metal powder is practiced to concentrate the Pd. Dissolution of the cemented Pd metal is necessary to recover pure Pd metal or compounds. In this work, the leaching behavior of Pd metal in inorganic acid solutions (hydrochloric..... More

                   Web of Science 7  Crossref 7
Adsorption of Pd(II) onto Zr(IV) Based Metal-Organic Framework UIO-66-NH<sub>2</sub> from Hydrochloric Acid Solution
염산 용액에서 지르코늄(IV)계 금속-유기물 구조체 UIO-66-NH2의 팔라듐(II) 흡착
Hyeong Hun Ahn, Man Seung Lee
안형훈, 이만승
Korean J. Met. Mater. 2019;57(9):589-595.   Published online 2019 Aug 21
DOI: https://doi.org/10.3365/KJMM.2019.57.9.589

Abstract
Metal-organic frameworks are used in many applications, such as gas separation, catalysis, and the synthesis of nanomaterials. Metal-organic frameworks show superior stability at high temperature, which makes them potentially useful for the adsorption of metal ions from leaching solutions at high temperature. In this work, UIO-66-NH2, a zirconium(IV) based metal-organic..... More

                   Web of Science 1  Crossref 1
Separation and Recovery of Precious Metals from Leach Liquors of Spent Electronic Wastes by Solvent Extraction
Thi Hong Nguyen, Lingyun Wang, Man Seung Lee
Korean J. Met. Mater. 2017;55(4):247-255.   Published online 2017 Apr 6
DOI: https://doi.org/10.3365/KJMM.2017.55.4.247

Abstract
Solvent extraction was employed to recover precious metals (Au (III), Pd (II) and Pt (IV)) from the leach solution of spent electronic wastes containing Cu (II), Cr (III) and Fe (III). First, pure Fe (III) and Au (III) were recovered by simultaneous extraction with Cyanex 923 followed by selective stripping..... More

       Crossref 16
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